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Beilstein J. Org. Chem. 2012, 8, 1523–1527, doi:10.3762/bjoc.8.172
Graphical Abstract
Figure 1: The chemical structures of DMP (1), 2-iodobenzoic acid (2), IBX (3) and 4.
Figure 2: ORTEP diagram (50% probability level) of 1 with numbering scheme.
Figure 3: Supramolecular structure of 1 with halogen bonds and selected hydrogen bonds.
Figure 4: Further hydrogen-bond interactions in the supramolecular structure of 1.
Figure 5: Supramolecular structure of 1 viewed along axis b.